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Optimizing Distillation Tower Parameters to Reduce Free Fatty Acid Content in Palm Kernel Oil Exports
2026-01-12
QI ' E Group
Application Tips
The distillation tower is a critical component in enhancing the quality of palm kernel oil, particularly in reducing the content of free fatty acids. This paper delves into the technical differences between vacuum distillation and molecular distillation, elaborates on the impact of three core parameters - temperature gradient, vacuum degree, and residence time - on free fatty acid residues, and reveals common operational pitfalls and scientific countermeasures. It aims to assist technicians in precisely controlling the process, significantly improving the pass - rate and added value of the oil products.

1. Introduction: Addressing the Pain Points

As a palm kernel oil exporter, you may have received feedback from customers complaining about issues like strong odor and high acid value in the oil. These problems are directly related to the high content of free fatty acids (FFAs) in the product. High FFA levels not only affect the quality and taste of the oil but also reduce its market value. For instance, the industry standard AOCS (American Oil Chemists' Society) has set strict limits on the FFA content for palm kernel oil exports. If your product fails to meet these standards, it can lead to customer dissatisfaction and potential loss of business.

2. Technology Comparison: Vacuum Distillation vs. Molecular Distillation

When it comes to reducing the FFA content in palm kernel oil, two main distillation technologies are commonly used: vacuum distillation and molecular distillation. Each has its own unique features in terms of application scenarios, energy consumption, and equipment requirements.

Vacuum Distillation: This is a more traditional method. It is suitable for large - scale production with relatively low equipment investment. However, it has higher energy consumption. The energy consumption of a typical vacuum distillation system can be around 15 - 20 kWh per ton of palm kernel oil processed. It operates under a relatively high vacuum, usually between 1 - 10 mbar. The equipment is relatively simple and easy to maintain, but it may not be as effective in removing FFAs as molecular distillation in some cases.

Molecular Distillation: This advanced technology is more suitable for high - quality palm kernel oil production. It has lower energy consumption, about 10 - 15 kWh per ton of oil processed. Molecular distillation can operate at a very high vacuum, below 0.1 mbar, which allows for more efficient separation of FFAs. However, the equipment is more expensive and requires more professional operation and maintenance.

3. Parameter Details

Temperature Gradient: The temperature gradient in the distillation tower plays a crucial role in the decomposition of fatty acids. A proper temperature gradient can promote the evaporation of FFAs. If the temperature is too low, the FFAs may not evaporate effectively, resulting in high FFA residues. For example, in a well - designed distillation process, the temperature at the top of the tower should be around 150 - 160°C, while at the bottom, it can reach 200 - 210°C. A steep temperature gradient can accelerate the decomposition of FFAs, but it may also cause some side reactions if not controlled properly.

Vacuum Fluctuation: Vacuum fluctuation can cause oxidation of the oil. If the vacuum is not stable, oxygen may enter the system, leading to the oxidation of FFAs and other components in the oil. This can increase the acid value and produce unpleasant odors. A stable vacuum should be maintained within a narrow range, for example, with a fluctuation of no more than ±0.5 mbar.

Residence Time: If the residence time of the oil in the distillation tower is too long, it can increase the risk of side reactions. For example, long - term exposure to high temperatures may cause the polymerization of some fatty acids, which can affect the quality of the oil. The optimal residence time should be controlled within 10 - 15 minutes.

4. Common Mistakes and Corrective Measures

Mistake: Assuming Higher Vacuum is Always Better Many operators think that the higher the vacuum in the distillation tower, the better the separation effect. However, in reality, an overly high vacuum can cause some problems. For example, it may increase the energy consumption and also cause the oil to foam, which can affect the normal operation of the equipment. The corrective measure is to set the vacuum according to the specific requirements of the distillation process, usually within the range mentioned above.

Mistake: Ignoring Temperature Uniformity Inadequate temperature control can lead to uneven decomposition of FFAs. To correct this, a well - designed temperature control system should be installed to ensure a uniform temperature gradient throughout the distillation tower.

5. Practical Operation Process and Check List

Operation Process: First, select the appropriate distillation technology according to your production scale and quality requirements. Then, set the temperature gradient, vacuum degree, and residence time based on the characteristics of the palm kernel oil. During the operation, monitor the key parameters continuously and make timely adjustments if necessary. After the distillation is completed, conduct a quality inspection of the oil to ensure that the FFA content meets the standards.

Check List:

  • Check the vacuum system for leaks before starting the operation.
  • Verify the accuracy of the temperature sensors and control valves.
  • Ensure that the residence time is within the set range.
  • Regularly clean the condensers and other equipment to prevent blockages.

6. Conclusion and Call - to - Action

By understanding and controlling the key parameters of the distillation tower, you can effectively reduce the FFA content in palm kernel oil, improve the quality of the product, and increase its market competitiveness. If you want to have a more in - depth understanding of the palm kernel oil distillation process, we have prepared a valuable resource for you. If you need the "Comparison Table of Palm Kernel Oil Distillation Process Parameters", welcome to leave a message [Distillation] to get the PDF version. Please feel free to share this article with your colleagues and friends in the industry and save it for future reference. Leave a comment below if you have any questions or need more information!

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